Table 1 Intraday precision and accuracy (a) and (b) interday precision and accuracy
a. Intraday precision and accuracy | ||||
|---|---|---|---|---|
Spiked concentration (ng/ml) | Average fluralaner concentration (n = 5) | Standard deviation (ng/ml) | Relative standard deviation (RSD %) | Average accuracy (%) |
5 | 5 | 0.4 | 7.4 | 98.2 |
10 | 10 | 0.3 | 2.6 | 103.6 |
50 | 44 | 2.9 | 6.5 | 88.7 |
1000 | 1088 | 47.4 | 4.4 | 108.8 |
b. Interday precision and accuracy | ||||
|---|---|---|---|---|
Spiked concentration (ng/ml) | Average fluralaner concentration (n = 7) | Standard deviation (ng/ml) | Relative standard deviation (RSD %) | Average accuracy (%) |
5 | 5 | 0.5 | 9.8 | 101.0 |
10 | 9 | 0.3 | 3.6 | 94.3 |
50 | 49 | 1.2 | 2.5 | 98.5 |
100 | 99 | 5.8 | 5.8 | 99.2 |
500 | 524 | 39.3 | 7.5 | 104.8 |
1000 | 1008 | 60.8 | 6.0 | 100.8 |